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HRID2046

反应详情

EQUATION

反应方程式

HRID 2046 的结构方程式

REACTANTS

反应物

2
结构：CP(C)(=O)CCl
HCID74224

Phosphine oxide, (chloromethyl)dimethyl-

C3H8ClOP

结构：Cn1c(Br)nc2c1c(=O)[nH]c(=O)n2C.[Na]
HCID67653895

未命名化合物

PRODUCTS

生成物

1
结构：Cn1c(Br)nc2c1c(=O)n(CP(C)(C)=O)c(=O)n2C
HCID19689193

未命名化合物

PROCEDURE

实验过程

The title substance was prepared from 28 g (0.1 mol) of 8-bromo-3,7-dimethylxanthine sodium salt and chloromethyldimethylphosphine oxide analogously to Example 59 and chromatographed on silica gel.

WORKUP

后处理

  1. customchromatographed on silica gel