HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-diethyl 4-iodo-1H-pyrazole-3,5-dicarboxylate → 1-(2-tert-Butoxycarbonylamino-ethyl)-4-iodo-1H-pyrazole-3,5-dicarboxylic acid diethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-diethyl 4-iodo-1H-pyrazole-3,5-dicarboxylate | HCID 11739230 | — |
| Reactant | 2-(2-tert-Butoxycarbonylamino-ethyl)-5-phenoxymethyl-2H-pyrazole-3-carboxylic acid ethyl ester | HCID 67958224 | — |
| Product | 1-(2-tert-Butoxycarbonylamino-ethyl)-4-iodo-1H-pyrazole-3,5-dicarboxylic acid diethyl ester | HCID 67975816 | — |
Reaction Steps
The compound was prepared from 4-iodo-1H-pyrazole-3,5-dicarboxylic acid diethyl ester and 2-(2-tert-butoxycarbonylamino)ethyl bromide using the method described in the preceding example 5 (2-(2-tert-butoxycarbonylamino-ethyl)-5-phenoxymethyl-2H-pyrazole-3-carboxylic acid ethyl ester).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592422B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-f42d332cd7b6453a8beec81efeb796c8 |
| Source note | uspto-grants-2013_11 |