HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → 2-Acetyl-5-p-tolyl-cyclohexane-1,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 5-(4-Methylphenyl)cyclohexane-1,3-dione | HCID 576492 | — |
| Reactant | 2-Acetyl-5-(4-fluoro-phenyl)cyclohexane-1,3-dione | HCID 52950883 | — |
| Product | 2-Acetyl-5-p-tolyl-cyclohexane-1,3-dione | HCID 58269411 | — |
Reaction Steps
The title compound was prepared from 5-p-tolyl-cyclohexane-1,3-dione (1.6 g, 5.74 mmol), from example 1/c stage 2, and sodium acetate (470 mg, 5.74 mmol), following the procedure describing the synthesis of 2-acetyl-5-(4-fluoro-phenyl)-cyclohexane-1,3-dione (example 3/a stage 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592430B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-6a9b5b31d77b4c3ea27469049e93bf4e |
| Source note | uspto-grants-2013_11 |