HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → 2-Acetyl-5-(2-methoxyphenyl)cyclohexane-1,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 5-(2-Methoxyphenyl)-1,3-cyclohexanedione | HCID 17122313 | — |
| Reactant | 2-Acetyl-5-(4-fluoro-phenyl)cyclohexane-1,3-dione | HCID 52950883 | — |
| Product | 2-Acetyl-5-(2-methoxyphenyl)cyclohexane-1,3-dione | HCID 18317352 | — |
Reaction Steps
The title compound was prepared from 5-(2-methoxy-phenyl)-cyclohexane-1,3-dione (1.0 g, 4.58 mmol), example 1/a, and sodium acetate (376 mg, 4.58 mmol), following the procedure describing the synthesis of 2-acetyl-5-(4-fluoro-phenyl)-cyclohexane-1,3-dione (example 3/a stage 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592430B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-2bf71919d38b483d98f2647d008e4ff5 |
| Source note | uspto-grants-2013_11 |