HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 76750917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 76750935 | HCID 76750935 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 76750917 | HCID 76750917 | — |
Reaction Steps
The title compound was prepared from (2-amino-7-biphenyl-2-yl-4-methyl-7,8-dihydro-6H-quinazolin-5-ylideneaminooxy)-acetic acid (compound 69) by treating with thionyl chloride followed by amidation using morpholine and triethylamine in DCM.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592430B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-e5cba02108e84063979af4184a9bdc86 |
| Source note | uspto-grants-2013_11 |