HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 60141184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 60141183 | HCID 60141183 | — |
| Product | HCID 60141184 | HCID 60141184 | — |
Reaction Steps
In analogy to the procedure described for the preparation of intermediate A-11 [C], (1-{(rac)-3-[5-chloro-3-fluoro-2-(2-methyl-2H-tetrazol-5-yl)-phenyl]-6,7-dihydro-5H-[1]pyrindin-7-ylcarbamoyl}-cyclopropyl)-carbamic acid tert-butyl ester (example 54) has been treated with trifluoroacetic acid (90%) to give the title compound as light brown amorphous solid. MS: 428.1 (MH+, 1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592426B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-34615787032344ee8007e2804f63d12d |
| Source note | uspto-grants-2013_11 |