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HRID2046682

反应详情

EQUATION

反应方程式

HRID 2046682 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[Li+].[Li+]
HCID11125

Lithium carbonate

CLi2O3

结构：COc1c(F)c(F)cc(C#N)c1F
HCID14096370

2,4,5-Trifluoro-3-methoxybenzonitrile

C8H4F3NO

结构：C[C@@H]1NCC[C@@H]1C(C)(C)O
HCID55299039

未命名化合物

PRODUCTS

生成物

1
结构：COc1c(F)c(C#N)cc(F)c1N1CC[C@H](C(C)(C)O)[C@@H]1C
HCID59370542

未命名化合物

PROCEDURE

实验过程

Using 2,4,5-trifluoro-3-methoxybenzonitrile (347 mg), (2S,3S)-3-(1-hydroxy-1-methylethyl)-2-methylpyrrolidine 1/2 oxalate (409 mg) and lithium carbonate (328 mg), the title compound was obtained as a pale-yellow oil (yield: 175 mg) by an operation similar to that in Example 3.