HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Carbonate → HCID 16066094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Carbonate | HCID 11125 | — |
| Reactant | 4-Fluoro-3-(trifluoromethyl)benzonitrile | HCID 144255 | — |
| Reactant | HCID 68603378 | HCID 68603378 | — |
| Product | HCID 16066094 | HCID 16066094 | — |
Reaction Steps
Using 4-fluoro-3-(trifluoromethyl)benzonitrile (398 mg), 0.9 mol/L (2S,3S)-2-methylpyrrolidin-3-ol dimethyl sulfoxide solution (2.35 mL) and lithium carbonate (156 mg), the title compound was obtained as yellow crystals (yield: 135 mg) by an operation similar to that in Example 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592452B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-f4596f8980ec4ec8a6fe72feaa21252a |
| Source note | uspto-grants-2013_11 |