HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichlorobenzaldehyde → (5-bromo-1H-pyrrolo[2,3-b]pyridin-3-yl)-(2,6-dichlorophenyl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichlorobenzaldehyde | HCID 6737 | — |
| Reactant | (5-bromo-1H-pyrrolo[2,3-b]pyridin-3-yl)(2,6-dichloro-3-fluorophenyl)methanol | HCID 67004517 | — |
| Product | (5-bromo-1H-pyrrolo[2,3-b]pyridin-3-yl)-(2,6-dichlorophenyl)methanol | HCID 67004341 | — |
Reaction Steps
Prepared according to the method described above for synthesis of (5-bromo-1H-pyrrolo[2,3-b]pyridin-3-yl)-(2,6-dichloro-3-fluorophenyl)methanol, using 2,6-dichloro-benzaldehyde. MS (ES+): m/z 370.85, 372.85, 374.83 [MH+]; HPLC: tR=3.25 min (ZQ3, polar—5 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592448B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-ee717b16af8f40728480a6d89d4a3669 |
| Source note | uspto-grants-2013_11 |