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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2047142Generated: October 30, 2026

1,1'-Carbonyldiimidazole → HCID 66733615, compound

https://huagongshe.com/reaction/2047142

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,1'-CarbonyldiimidazoleHCID 68263—
ReactantHCID 66733484HCID 66733484—
SolventTetrahydrofuranHCID 8028—
ProductHCID 66733615HCID 66733615—

Reaction Steps

To a solution of (R)-2-(benzyloxy)propanehydrazide (194 mg, 1 mmol) in anhydrous THF (2 mL) was added CDI (178 mg, 1.1 mmol) and the resulting mixture was allowed to stir one hour. Solvent was removed under reduced pressure and the residue was purified on silica gel. Elution with EtOAc yielded title product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08591943B2
Source datasetuspto-grants-2013_11
ORD IDord-47cf6f7ebde240dc92b2aef5f4395461
Source noteuspto-grants-2013_11