HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrazol-3-ylamine → HCID 66735271, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrazol-3-ylamine | HCID 74561 | — |
| Reactant | HCID 57891190 | HCID 57891190 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 66735271 | HCID 66735271 | — |
Reaction Steps
The crude tert-butyl 4-(3-cyano-2-oxopropyl)piperidine-1-carboxylate was then heated at 100° C. overnight with 1H-pyrazol-5-amine (1197 mg, 14.41 mmoL) in HOAc (25 mL). Concentration provided crude tert-butyl 4-((7-aminopyrazolo[1,5-a]pyrimidin-5-yl)methyl)piperidine-1-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08591943B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-21b2928d13c5471cb8a26a5bd8b4f95d |
| Source note | uspto-grants-2013_11 |