HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Diethylamino)-6-methylisonicotinic acid → HCID 68578316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Diethylamino)-6-methylisonicotinic acid | HCID 58418055 | — |
| Reactant | HCID 178436622 | HCID 178436622 | — |
| Product | HCID 68578316 | HCID 68578316 | — |
Reaction Steps
The title compound is prepared in analogy to Example 5 starting from N-[2-ethyl-4-(N-hydroxycarbamimidoyl)-phenyl]-acetamide and 2-diethylamino-6-methyl-isonicotinic acid; LC-MS: tR=0.81 min, [M+1]+=394.15; 1H NMR (CDCl3): δ 1.25 (t, J=7.0 Hz, 6H), 1.36 (t, J=7.3 Hz, 3H), 2.28 (s, 3H), 2.50 (s, 3H), 2.73 (q, J=7.3 Hz, 2H), 3.63 (q, J=6.8 Hz, 4H), 7.01 (s, 1H), 7.08-7.16 (m, 2H), 8.03-8.09 (m, 2H), 8.13-8.21 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592460B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-a4d0420c31cf41a7b98e2b7a20c0861d |
| Source note | uspto-grants-2013_11 |