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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2047401Generated: October 31, 2026

Dichloromethane → HCID 68671994, compound

https://huagongshe.com/reaction/2047401

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethaneHCID 6344—
ReactantHCID 68671384HCID 68671384—
SolventHydrochloric AcidHCID 313—
SolventMethanolHCID 887—
SolventDiethyl EtherHCID 3283—
ProductHCID 68671994HCID 68671994—

Reaction Steps

To a mixture of {1-[3-(1-Methyl-1H-benzoimidazol-2-yl)-phenyl]-piperidin-4-yl}-carbamic acid tert-butyl ester (2.00 g, 4.93 mmol) in dichloromethane (2 mL) and methanol (1 mL), 2M HCl in Et2O (25 mL) was added and the resulting mixture was stirred overnight at room temperature.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08592463B2
Source datasetuspto-grants-2013_11
ORD IDord-87f58435edd54ac290c543d26bf66ab0
Source noteuspto-grants-2013_11