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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2047530Generated: November 1, 2026

HCID 178452023, compound → HCID 178494068, compound

https://huagongshe.com/reaction/2047530

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178452023HCID 178452023—
ReactantHCID 178494069HCID 178494069—
ProductHCID 178494068HCID 178494068—

Reaction Steps

The title compound was prepared according to the procedure described in Example 38C, substituting the product of Example 39A for the product of Example 38B. 1H NMR (500 MHz, CDCl3) δ ppm 8.77 (s, 2H) 8.05 (d, J=8.54 Hz, 1H) 7.97 (s, 1H) 7.58 (dd, J=8.54, 1.83 Hz, 1H) 4.08 (s, 3H) 3.85-3.98 (m, 1H) 3.60-3.70 (m, 1H) 3.08-3.16 (m, 1H) 2.90-3.02 (m, 2H) 2.73-2.81 (m, 1H) 2.61-2.71 (m, 2H) 2.49-2.60 (m, 3H) 2.31-2.47 (m, 3H) 1.93-2.05 (m, 1H) 1.58-1.74 (m, 1H). MS: (M+H)+=408.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08592467B2
Source datasetuspto-grants-2013_11
ORD IDord-57cfd744b088423c918d5dbe15d64653
Source noteuspto-grants-2013_11