HCID 86655961, compound → (Z)-Benzaldehyde oxime

Participants

Reaction Steps

A 1.5 mol/L methanesulfonyl chloride/N-methylpyrrolidone solution was sent as a first fluid from the center at a ratio of supply pressure/back pressure of 0.10 MPa/0.03 MPa, a rotation speed of 1000 rpm, and a sending temperature of 25° C., and a 1.0 mol/L benzaldoxime/N-methylpyrrolidone solution was introduced as a second fluid into a space between the processing surfaces at 20 mL/min. The first fluid and the second fluid were mixed in a thin film fluid, and then a solution obtained after processing was discharged from the space between the processing surfaces at 44 mL/min. As a result of HPLC analysis, substantially complete conversion of benzaldoxime to benzonitrile was observed.

Provenance & Evidence