HCID 85722021, compound → Acetanilide

Participants

Reaction Steps

A 0.15 mol/L methanesulfonyl chloride/pyridine solution was sent as a first fluid from the center at a ratio of supply pressure/back pressure of 0.15 MPa/0.07 MPa, a rotation speed of 500 rpm, and a sending temperature of 25° C., and a 0.1 mol/L acetophenone oxime/pyridine solution was introduced as a second fluid into a space between the processing surfaces at 30 mL/min. The first fluid and the second fluid were mixed in a thin film fluid, and then a solution obtained after processing was discharged from the space between the processing surfaces at 58 mL/min. As a result of HPLC analysis, substantially complete conversion to acetanilide was observed.

Provenance & Evidence