HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-2-butanol → 2-Methyl-2-butanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-2-butanol | HCID 6405 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Product | 2-Methyl-2-butanol | HCID 6405 | — |
| Product | Sodium t-amyl oxide | HCID 70700164 | — |
Reaction Steps
Tert-amyl alcohol was sent as a first fluid from the center at a ratio of supply pressure/back pressure of 0.40 MPa/0.25 MPa, a rotation speed of 1000 rpm, and a sending temperature of 120° C., and sodium was introduced as a second fluid at 103° C. into a space between the processing surfaces at 10 mL/min. The first fluid and the second fluid were mixed in a thin film fluid, and then a solution obtained after processing was discharged from the space between the processing surfaces at 19 mL/min. As a result, a solution of sodium t-amyl oxide and t-amyl alcohol was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592498B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-f868dfb769114d7b98511b8ee5e5e3c0 |
| Source note | uspto-grants-2013_11 |