2-Methyl-2-butanol → 2-Methyl-2-butanol

HRID 2047581Notes

Reaction equation

HRID 2047581 reaction equation
[C:1]([OH:6])([CH2:4][CH3:5])([CH3:3])[CH3:2].[Na:7]>>[C:1]([O:6][C:1]([CH2:4][CH3:5])([CH3:3])[CH3:2])([CH2:4][CH3:5])([CH3:3])[CH3:2].[Na:7].[C:1]([OH:6])([CH2:4][CH3:5])([CH3:3])[CH3:2]

Participants

4

Reactant 2

HCID 64052-Methyl-2-butanolHCID 5360545Sodium

Product 2

HCID 64052-Methyl-2-butanolHCID 70700164Sodium t-amyl oxide

Procedure

Tert-amyl alcohol was sent as a first fluid from the center at a ratio of supply pressure/back pressure of 0.40 MPa/0.25 MPa, a rotation speed of 1000 rpm, and a sending temperature of 120° C., and sodium was introduced as a second fluid at 103° C. into a space between the processing surfaces at 10 mL/min. The first fluid and the second fluid were mixed in a thin film fluid, and then a solution obtained after processing was discharged from the space between the processing surfaces at 19 mL/min. As a result, a solution of sodium t-amyl oxide and t-amyl alcohol was obtained.

Workup

  1. additionThe first fluid and the second fluid were mixed in a thin film fluid
  2. customa solution obtained after processing

Sources & evidence

ORD record
ord-f868dfb769114d7b98511b8ee5e5e3c0
Source dataset
uspto-grants-2013_11
Patent number
US08592498B2

Reaction notes

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