HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 44596058, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethanone, 2-amino-1-phenyl-, hydrochloride (1:1) | HCID 2723597 | — |
| Reactant | HCID 67182730 | HCID 67182730 | — |
| Solvent | Isoamyl Alcohol | HCID 31260 | — |
| Product | HCID 44596058 | HCID 44596058 | — |
Reaction Conditions
| Temperature | 120 °C |
|---|
Reaction Steps
To a suspension of 0.12 g (0.51 mmol) of 1-Methyl-6-methylsulfanyl-4-pyridin-4-yl-1H-[1,3,5]triazin-2-one in 1 mL of 3-methyl-1-butanol was added 0.088 g (0.51 mmol) of 2-Amino-1-phenyl-ethanone hydrochloride (commercially available). To the resulting mixture was added 7.1 mg (0.051 mmol) of potassium carbonate. The resulting mixture was stirred at 120° C. for 1 h. Then, 7.1 mg (0.051 mmol) of potassium carbonate were added each hour during 2 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592580B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-fad381bdde4d491388180807985e5293 |
| Source note | uspto-grants-2013_11 |