HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → HCID 67182730, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 178503394 | HCID 178503394 | — |
| Product | HCID 67182730 | HCID 67182730 | — |
Reaction Steps
By analogy with the method described in example 1 (step 1.2), using benzylamine (commercially available) in place of phenethylamine and 6-Methylsulfanyl-4-pyridin-4-yl-1H-[1,3,5]triazin-2-one (synthesis as described in U.S. Pat. No. 4,406,897) in place of 1-Methyl-6-methylsulfanyl-4-pyridin-4-yl-1H-[1,3,5]triazin-2-one, to afford the product which was transformed into the hyrdochloride salt in the usual manner to give 0.15 g (47%) of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592580B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-8d14367b23894262b88c8da607b34461 |
| Source note | uspto-grants-2013_11 |