Diethyl (ethoxymethylene)malonate → HCID 178469592, compound

HRID 2047724Notes

Reaction equation

HRID 2047724 reaction equation
[CH:1]([O:4][C:5]1[CH:11]=[CH:10][C:8]([NH2:9])=[CH:7][CH:6]=1)([CH3:3])[CH3:2].C([O:14][CH:15]=[C:16]([C:22](OCC)=O)[C:17]([O:19][CH2:20][CH3:21])=[O:18])C>>[OH:14][C:15]1[C:10]2[C:8](=[CH:7][CH:6]=[C:5]([O:4][CH:1]([CH3:3])[CH3:2])[CH:11]=2)[N:9]=[CH:22][C:16]=1[C:17]([O:19][CH2:20][CH3:21])=[O:18]

Participants

3

Reactant 2

HCID 6871Diethyl (ethoxymethylene)malonateHCID 821124-Isopropoxyaniline

Product 1

HCID 178469592HCID 178469592, compound

Procedure

Prepared as in Example 1c from 4-isopropoxyaniline and diethyl 2-(ethoxymethylene)malonate as a yellow solid (20%). MS 276 (MH+).

Sources & evidence

ORD record
ord-5bc0780fc6fb47d39b200fb2d0d55e54
Source dataset
uspto-grants-2013_11
Patent number
US08592592B2

Reaction notes

Loading…