HRID2048129

反应详情

EQUATION

反应方程式

REACTANTS

反应物

$结构：CC(C)(C)OC(=O)N1CCC(C(=O)N/N=C(\N)c2ccccn2)CC1$

HCID87242610

未命名化合物

PRODUCTS

生成物

结构：CC(C)(C)OC(=O)N1CCC(c2n[nH]c(-c3ccccn3)n2)CC1

HCID178451825

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

2 次

CONDITIONS

反应条件

温度: 150 °C

PROCEDURE

实验过程

Tert-butyl 4-({(2Z)-2-[amino(pyridin-2-yl)methylidene]hydrazinyl}carbonyl)piperidine-1-carboxylate 45 g (129 mM) obtained in step II is melted at 220° C. under nitrogen atmosphere for 1 hr. Reaction is then cooled to 150° C. and added ethanol till solid get dissolved. Ethanol is then evapourated to get desired compound.

WORKUP

后处理

customfor 1 hr
customReaction
customget
dissolutiondissolved