HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2048129Generated: October 30, 2026
tert-butyl 4-[[(Z)-[amino(pyridin-2-yl)methylidene]amino]carbamoyl]piperidine-1-carboxylate → HCID 178451825, compound
https://huagongshe.com/reaction/2048129
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | tert-butyl 4-[[(Z)-[amino(pyridin-2-yl)methylidene]amino]carbamoyl]piperidine-1-carboxylate | HCID 87242610 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178451825 | HCID 178451825 | — |
Reaction Steps
Tert-butyl 4-({(2Z)-2-[amino(pyridin-2-yl)methylidene]hydrazinyl}carbonyl)piperidine-1-carboxylate 45 g (129 mM) obtained in step II is melted at 220° C. under nitrogen atmosphere for 1 hr. Reaction is then cooled to 150° C. and added ethanol till solid get dissolved. Ethanol is then evapourated to get desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08592591B2 |
|---|
| Source dataset | uspto-grants-2013_11 |
|---|
| ORD ID | ord-6f82ff686d974c87b1b6bb3c92e20161 |
|---|
| Source note | uspto-grants-2013_11 |
|---|
