HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 67028257, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 86631774 | HCID 86631774 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67028257 | HCID 67028257 | — |
Reaction Steps
To the stirred solution 4-(6-bromo-3-phenylimidazo[1,2-a]pyridin-2-yl)benzaldehyde (0.795 mM) in 15 mL of methanol is added NaBH4 (1.5 eq) at 0° C. and the reaction is allowed to stir at room temperature for 1 hr. The reaction is concentrated and quenched with water. The precipitated solid is filtered and dried to yield the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592591B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-17ac05a9e61b4f0089ece533ca9ac0e9 |
| Source note | uspto-grants-2013_11 |