Ethanone, 1-(3,4-dichlorophenyl)- → HCID 86736902, compound

Participants

Reaction Steps

A solution of 5.0 g of 3', 4'-dichloroacetophenone in 50 ml of 90% ethanol was mixed with 2.4 g of aminooxyacetamide and subsequently boiled. The solvent was removed in a vacuum and the residue was extracted with chloroform. The chloroform solution was washed thrice with water, dried over anhydrous sodium sulfate and subsequently concentrated by evaporation in a vacuum. After the addition of ether and petroleum ether the superscribed substance crystallized out from the concentrate. Melting point 111° C.-111.5° C.

Provenance & Evidence