HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Ethyl Ketone → HCID 85939531, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Ethyl Ketone | HCID 6569 | — |
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Phenol dibromide | HCID 20345032 | — |
| Product | HCID 85939531 | HCID 85939531 | — |
Reaction Steps
There was kept under reflux for 6 hours 300 ml of methylethylketone containing 21 g of the phenol of step (A), 15 g of potassium carbonate and 18 g of ethylbromoacetate. After hot filtration the solvent was evaporated and the solid recrystallised in ethanol. 21 g of the ester were obtained, which melted at 114° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04197309 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-55aee60d737a4efd80056fb1bc3e179f |
| Source note | uspto-grants-1980_04 |