HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-(5-Chlorothiophen-2-yl)-3-oxopropanenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 70567245 | HCID 70567245 | — |
| Product | 3-(5-Chlorothiophen-2-yl)-3-oxopropanenitrile | HCID 12540181 | — |
Reaction Steps
A 9.2 g. portion of β-amino-5-chloro-2-thiopheneacrylonitrile is dissolved in 100 ml. of methanol. A 50 ml. portion of 1 N hydrochloric acid is added and the mixture is stirred at room temperature for 3 hours. The precipitate is collected giving 5-chloro-β-oxo-2-thiophenepropionitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04197310 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-65d65e208a7f457abb20222f095b3e8f |
| Source note | uspto-grants-1980_04 |