HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 12796479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 86736929 | HCID 86736929 | — |
| Solvent | 1-Propanol | HCID 1031 | — |
| Product | HCID 12796479 | HCID 12796479 | — |
Reaction Steps
A refluxing solution (under nitrogen) of (Z)-2β-ethoxy-3α-hydroxy-5α-pregn-17(20)-en-11-one 11-oxime (450 mg) in propan-1-ol (15 ml) was treated with pieces of Na (450 mg). When there was no trace of Na left the mixture was added to chilled water to give a fine precipitate which was collected by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04197296 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-c5916c7df67241d0a978b165b9c129b0 |
| Source note | uspto-grants-1980_04 |