HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131711741, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-[(4-methylphenyl)sulfanyl]aniline | HCID 459376 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 131711741 | HCID 131711741 | — |
Reaction Steps
A solution of 2.8 g (0.04 mol) of sodium nitrite in 15 ml of water is added dropwise, at an internal temperature of max. 10° C., to 10.7 g (0.04 mol) of 4-(4-methylthiophenoxy)-aniline in 100 ml of glacial acetic acid and 7.5 ml of conc. hydrochloric acid. Then stirring is continued for 15 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198407 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-54f6a8d5244e46adbbfc772a4b2f3662 |
| Source note | uspto-grants-1980_04 |