HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20344096, compound → 2-(3-Fluorophenoxy)benzenemethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20344096 | HCID 20344096 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-(3-Fluorophenoxy)benzenemethanol | HCID 20344098 | — |
Reaction Steps
Ethyl 2-(3-fluorophenoxy)benzoate (37 g.) dissolved in 90 ml. of ether, was added dropwise to a suspension of lithium aluminum hydride (4.5 g.) in 350 ml of ether. The reaction mixture was heated to reflux for 6 hours to give, after work-up, 30 g. of the title compound. ##STR11##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198421 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-53aadc8e99ea495b91c79fd82f8b881d |
| Source note | uspto-grants-1980_04 |