HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiocyanic acid, chloromethyl ester → HCID 53691075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiocyanic acid, chloromethyl ester | HCID 76755 | — |
| Reactant | 4-Methylthiobenzoic acid | HCID 178425911 | — |
| Product | HCID 53691075 | HCID 53691075 | 80% |
Reaction Steps
20.5 g (0.11 mol) of the K salt of 4-methyl-thiobenzoic acid and 11.7 g (0.11 mol) of chloromethyl thiocyanate were reacted and processed as in Example 1 B. 22.5 g of a light powder resulted and, after recrystallisation from ligroin, 18 g of white crystals resulted; melting point 55° (this corresponds to a yield of 80% of the theoretical conversion).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198428 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-64c61d4a85004d3f84bae29f0ae93210 |
| Source note | uspto-grants-1980_04 |