HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20344070, compound → HCID 20344086, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20344070 | HCID 20344070 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20344086 | HCID 20344086 | — |
Reaction Steps
A solution of 5.0 g of 10,11-dihydro-1'-methyl-11-oxospiro[dibenz(b,f)thiepin-10,4'-piperidine], free base of Example 8, in 40 ml of tetrahydrofuran is treated according to the procedure of Example 7 to provide 10,11-dihydro-11-hydroxy-1'-methylspiro[dibenz(b,f)thiepin-10,4'-piperidine].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198420 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-6be04c30d9dc4c04b07c157347bc02d3 |
| Source note | uspto-grants-1980_04 |