HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributylstannane → HCID 12878307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributylstannane | HCID 5948 | — |
| Reactant | HCID 12878297 | HCID 12878297 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 12878307 | HCID 12878307 | — |
Reaction Steps
The product obtained by reducing 2.0 g of 3-hydroxy-3-methyl-4-bromo-5-(p-benzyloxyphenyl)-5-pentanolide with 5.99 g of tri-n-butyltin hydride in 40 ml of anhydrous tetrahydrofuran according to the method described in Example 2 (a), was separated by a thin layer chromatography into two isomers in a total yield of 1.40 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198425 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-3de33ce29f194536825d6c03de10a85e |
| Source note | uspto-grants-1980_04 |