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HRID2049733

反应详情

EQUATION

反应方程式

HRID 2049733 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)CC(=O)c1ccccc1
HCID7166

1-Benzoylacetone

C10H10O2

结构：N#CC(N)c1ccccc1
HCID40838

未命名化合物

PRODUCTS

生成物

1
结构：Cc1[nH]c(-c2ccccc2)c(N)c1C(=O)c1ccccc1
HCID3042143

(4-amino-2-methyl-5-phenyl-1H-pyrrol-3-yl)-phenylmethanone

C18H16N2O

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC.CCOCC
溶剂HCID21584099

Diethylether hexane

C10H24O

PROCEDURE

实验过程

Starting from 2-amino-2-phenylacetonitrile and benzoylacetone, the open-chain intermediate compound is obtained, melting at 134°-135° C. (from diethyl ether/hexane). The title compound is obtained in a 60% overall yield. M.P. 285°-290° C. (from methanol/diethyl ether). The free base melts at 203°-5° C. (from methanol).

WORKUP

后处理

  1. customthe open-chain intermediate compound is obtained