HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Benzyl-3-chloroisoquinolin-1(2H)-one → 2-Benzyl-3-ethylthio-1-oxo-1,2-dihydroisoquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Benzyl-3-chloroisoquinolin-1(2H)-one | HCID 20344414 | — |
| Reactant | Sodium ethylsulfide | HCID 86736943 | — |
| Product | 2-Benzyl-3-ethylthio-1-oxo-1,2-dihydroisoquinoline | HCID 20344422 | — |
Reaction Steps
By following the same procedure as in Example 1 using 0.5 g. of 2-benzyl-3-chloro-1-oxo-1,2-dihydroisoquinoline and 0.6 g. of an aqueous solution of 20% sodium ethylsulfide, 0.37 g. of 2-benzyl-3-ethylthio-1-oxo-1,2-dihydroisoquinoline was obtained (recrystallized from cyclohexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198512 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-4e010d6f4897440699d8916fbed40a81 |
| Source note | uspto-grants-1980_04 |