HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenyl-1-propanone → HCID 54049612, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenyl-1-propanone | HCID 7148 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Catalyst | Boron trifluoride etherate | HCID 8000 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54049612 | HCID 54049612 | 62.2% |
Reaction Steps
In 30 ml of toluene, 2.68 g of propiophenone, 5.30 g of piperidine and 0.14 g of boron trifluoride etherate were dissolved. The mixture was treated in a manner similar to Example 1 to obtain 2.50 g of the desired enamine (yield: 50%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198510 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-18fc26d5417b4e33aba86803adf4dd8c |
| Source note | uspto-grants-1980_04 |