HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Chlorophenoxy)2-methyl-1-propene → 3-(4-Chlorophenoxy)-2-methyl-2-propene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Chlorophenoxy)2-methyl-1-propene | HCID 12409927 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-(4-Chlorophenoxy)-2-methyl-2-propene | HCID 20344578 | — |
Reaction Steps
Seven grams of 3-(4-chlorophenoxy)2-methyl-1-propene and 0.35 g of potassium t-butoxide are heated at 150° under nitrogen for 3 days. The mixture is then worked up with water and extracted with ether. The organic phase is washed with dilute acid, water and brine, dried over magnesium sulfate and solvent is removed to yield 3-(4-chlorophenoxy)-2-methyl-2-propene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198527 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-ec1071bd5aba40378722c6f082f079d4 |
| Source note | uspto-grants-1980_04 |