HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorophenol → Ethyl 3-phenoxyprop-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorophenol | HCID 7245 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl propiolate | HCID 12182 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Ethyl 3-phenoxyprop-2-enoate | HCID 237844 | — |
Reaction Steps
A solution of 5.77 mmol of ethyl propiolate in 20 ml ethyl ether is treated with 5.77 mmol 2-chlorophenol and 0.4 ml triethylamine (added slowly and with stirring). The reaction mixture is stirred overnight at RT, after which the solvent is removed under vacuum to yield ethyl 3-phenoxy-2-propenoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198527 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-975a1ad880cd4c5ca6ac7376a489e99a |
| Source note | uspto-grants-1980_04 |