HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23452868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 23452884 | HCID 23452884 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23452868 | HCID 23452868 | — |
Reaction Steps
A solution of crude (3,5-dicarbomethoxy-4-nitrophenoxy)-N,N-dihexylacetamide in ethanol is treated with aqueous sodium hydroxide (3 equivalents) at room temperature for 15 min. After this time the reaction is poured into cold dilute hydrochloric acid. The diacid product which precipitates is collected and washed well with water; m.p. 180°-184° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04199354 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-338b1f5c90354613af933c2dd6f0d6e2 |
| Source note | uspto-grants-1980_04 |