Hydrochloric Acid → HCID 23452868, compound

HRID 2049915Notes

Reaction equation

HRID 2049915 reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([CH:25]=[C:26]([C:31]([O:33]C)=[O:32])[C:27]=1[N+:28]([O-:30])=[O:29])[O:8][CH2:9][C:10]([N:12]([CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])=[O:11])([O:3]C)=[O:2].[OH-].[Na+].Cl>C(O)C>[C:31]([C:26]1[CH:25]=[C:7]([CH:6]=[C:5]([C:1]([OH:3])=[O:2])[C:27]=1[N+:28]([O-:30])=[O:29])[O:8][CH2:9][C:10]([N:12]([CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])=[O:11])([OH:33])=[O:32]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 14798Sodium HydroxideHCID 23452884HCID 23452884, compound

Product 1

HCID 23452868HCID 23452868, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of crude (3,5-dicarbomethoxy-4-nitrophenoxy)-N,N-dihexylacetamide in ethanol is treated with aqueous sodium hydroxide (3 equivalents) at room temperature for 15 min. After this time the reaction is poured into cold dilute hydrochloric acid. The diacid product which precipitates is collected and washed well with water; m.p. 180°-184° C.

Workup

  1. customThe diacid product which precipitates
  2. customis collected
  3. washwashed well with water

Sources & evidence

ORD record
ord-338b1f5c90354613af933c2dd6f0d6e2
Source dataset
uspto-grants-1980_04
Patent number
US04199354

Reaction notes

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