Water → Acetamide, N-(4,5,6,7-tetrahydro-7-oxobenzo[b]thien-4-yl)-

https://huagongshe.com/reaction/2049923

Participants

Role	Name	HCID	Charge
Reactant	Water	HCID 962	—
Reactant	N-(4,5,6,7-Tetrahydrobenzo[b]thiophen-4-yl)acetamide	HCID 4976773	—
Product	Acetamide, N-(4,5,6,7-tetrahydro-7-oxobenzo[b]thien-4-yl)-	HCID 106675	—

Reaction Conditions

Temperature	60 °C

Reaction Steps

Into a 100 ml, three necked round bottomed flask is placed 2.0 g of N-(4,5,6,7-tetrahydrobenz[b]-thien-4-yl)acetamide, 15 ml of H2O, and 31.5 ml of a 1.3 M cobaltic acetate solution prepared as in Example II. The mixture is stirred and heated to 60° C. under N2 for 12 hours and is worked up as in Example V. A material weighing 1.9 g and assaying as 76.8% of the product was obtained.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US04199510
Source dataset	uspto-grants-1980_04
ORD ID	ord-61a2f91be9414315b69759e95661976e
Source note	uspto-grants-1980_04