HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexane → HCID 22810729, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexane | HCID 8078 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Boc-N-Me-Phe-OH | HCID 7010602 | — |
| Reactant | HCID 18178029 | HCID 18178029 | — |
| Solvent | Cyclohexane ethylacetate | HCID 21867204 | — |
| Product | HCID 22810729 | HCID 22810729 | — |
Reaction Steps
This was prepared by coupling BOCMePheOH with N-methyl-3-methylthiopropylamine by the method of Example 1(b). The pure product was obtained after silica gel column chromatography in ethylacetate/cyclohexane (1:3). Rf=0.52 (ethylacetate:cyclohexane, 1:1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04199568 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-45af636307194515bb518f8440368329 |
| Source note | uspto-grants-1980_04 |