HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → 3-Methylthiopropan N-2-phenylethylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | Butanecarbothioyl chloride | HCID 22343826 | — |
| Product | 3-Methylthiopropan N-2-phenylethylamide | HCID 86736949 | — |
Reaction Steps
Prepared from 3-methylthiopropionyl chloride (2.76 g) and 2-phenylethylamine (5.04 g) by the method used in Example 10(a). The solid product (3.79 g) was pure by t.l.c. A sample crystallised from aqueous methanol as needles m.p. 56°-59°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04199568 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-2c699f3b86d548d88cacea4cb7971600 |
| Source note | uspto-grants-1980_04 |