HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20343343, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 54195762 | HCID 54195762 | — |
| Product | HCID 20343343 | HCID 20343343 | — |
Reaction Steps
To freshly distilled thionyl chloride (14.87 g, 0.125 mol) cooled in salt ice bath is added in portions the neopentyl alcohol of Example 36 (12.4 g, 0.05 mol) over 30 minutes. The ice bath is removed and the slurry is left to stand overnight. Evaporation of excess thionyl chloride gives a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04199595 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-9375e2ad4f22470ba9f380f69b4a3658 |
| Source note | uspto-grants-1980_04 |