HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Bis(methylthio)-2-nitroethylene → HCID 73677132, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Reactant | (3-Mercaptopropyl)ammonium chloride | HCID 197870 | — |
| Reactant | Propargylamine | HCID 239041 | — |
| Reactant | 1,3-Thiazol-2-ylmethanol | HCID 2795213 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | HCID 73677132 | HCID 73677132 | — |
Reaction Steps
When 2-hydroxymethylthiazole is reacted with 3-mercaptopropylamine hydrochloride [prepared according to the procedure described in J. Org. Chem., 27, 2846 (1962)] in aqueous hydrobromic acid (48%) and the resultant amine successively treated with 1,1-bis(methylthio)-2-nitroethylene and excess propargylamine, the title compound is produced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04200578 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-179bf7fcc3bd4cc29a30fe50b5ccb1ac |
| Source note | uspto-grants-1980_04 |