HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86736962, compound → HCID 23335809, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86736962 | HCID 86736962 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 23335809 | HCID 23335809 | — |
Reaction Steps
A solution of 3-[(acetyloxy)methyl]-7-[[2-carboxy-2-(1H-indol-1-yl)acetyl]amino]-8-oxo-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid, tert-butyl ester (0.05 mole) in 10 ml of trifluoroacetic acid maintained at 0° C. is stirred for 10 minutes. The trifluoroacetic acid is removed under vacuum. The residue is treated with ethyl ether to give a solid material. Filtration gives the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04200747 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-e04a2abe4f104046b2e45fcf50884427 |
| Source note | uspto-grants-1980_04 |