HRID2050392

反应详情

EQUATION

反应方程式

HRID 2050392 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A suspension of 0.499 g (1.81 mmole) of cis-2-azidomethyl-4-oxo-3-phenoxyacetylaminoazetidine and 0.189 g of 10% palladium on carbon in 25 ml of absolute ethanol was hydrogenated at atmospheric pressure and at 40° for 1 hour. The solution was filtered through celite and the solvent was removed in vacuo to afford the title compound as a colorless gum.

WORKUP

后处理

  1. filtrationThe solution was filtered through celite
  2. customthe solvent was removed in vacuo