HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86734330, compound → cis-2-Aminomethyl-4-oxo-3-phenoxyacetylaminoazetidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86734330 | HCID 86734330 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | cis-2-Aminomethyl-4-oxo-3-phenoxyacetylaminoazetidine | HCID 70593118 | — |
Reaction Steps
A suspension of 0.499 g (1.81 mmole) of cis-2-azidomethyl-4-oxo-3-phenoxyacetylaminoazetidine and 0.189 g of 10% palladium on carbon in 25 ml of absolute ethanol was hydrogenated at atmospheric pressure and at 40° for 1 hour. The solution was filtered through celite and the solvent was removed in vacuo to afford the title compound as a colorless gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04200572 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-86f832a4941d43b1a9d4d2c1e18e7a04 |
| Source note | uspto-grants-1980_04 |