Chlorokojic acid → HCID 88436748, compound

Participants

Reaction Steps

Chlorokojic acid (5 mmol) and 4-methylthiopyrimidine (5 mmol) were stirred at 170° C. for 10 minutes. The mixture melted, turned black, resolidified and was triturated with acetone to give as a crude solid, 1-(5-hydroxypyran-4-on-2-yl)-4-methylthiopyrimidinium chloride hydrochloride salt; (DMSO-d6)/130° C., 2.80(s,3H); 5.79(s,2H); 6.65(s,1H); 8.08(s,1H); 8.15(q,1H); 9.05(q,1H); 9.65(s,1H).

Provenance & Evidence