HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Chloromethyl)-6-methylpyridine → 1,3-Benzoxazole-2-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Chloromethyl)-6-methylpyridine | HCID 76546 | — |
| Reactant | Methyl 1,3-benzoxazole-2-carboxylate | HCID 13353743 | — |
| Product | 1,3-Benzoxazole-2-carbaldehyde | HCID 4483393 | 35% |
Reaction Steps
The title compound was prepared from methyl benzoxazole-2-carboxylate by the method of part (ii), above, on a 0.041 molar scale; yield 35% as a yellow oil. 1H-NMR(CDCl3)ppm(delta): 7.3-8.1 (m, 4H), 10.0 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05015473 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-54a6e228780d4e499b9a7031251577d4 |
| Source note | uspto-grants-1991_05 |